Nitrogen closed-cycle · solvent recovery

Closed-Loop Spray Dryer

A sealed spray dryer that uses nitrogen as the drying gas and condenses the evaporated solvent for reuse. Built for organic solvents, oxygen-sensitive products and explosion-proof duty.

Nitrogen loopSolvent recoveryExplosion-proofGMP
N₂Inert drying gas, recirculated
ClosedNo solvent vapour released
2014HMDS recovery plant, Shanxi Yangzhongxin
GMPDesigned to explosion-proof and GMP rules

How it works

Dry with nitrogen, condense the solvent, reuse both.

Nitrogen is heated and circulated through the drying tower. The feed is atomized into droplets that lose their solvent on contact with the hot gas. The gas then passes cyclones and a bag filter, and a condenser turns the solvent vapour back into liquid.

The non-condensable nitrogen is reheated and returned to the tower, so the system runs continuously without oxygen and without releasing solvent.

  • Oxidation-free drying with nitrogen
  • Recovers methanol, ethanol, acetone, hexane, ethyl and isopropyl acetate, dichloromethane
  • Explosion-proof sensors and control
  • Waste heat recovery and minimal emissions
Explosion-proof control unit, Yangzhongxin Material, 2014
Explosion-proof control unit, Yangzhongxin Material, 2014

Process

The closed nitrogen loop

  1. HeatA dedicated heater warms the nitrogen.
  2. AtomizeThe feed is pumped to a centrifugal atomizer.
  3. DryDroplets dry rapidly in the tower.
  4. SeparateCyclones and bag filters collect the powder.
  5. CondenseThe solvent is condensed and recovered as liquid.
  6. RecirculateNitrogen is reheated and reused.

Typical materials

Where closed-loop spray dryers are used

New materials

Precision ceramicsCarbide powdersHMDS

Batteries

Electrode materials in solvent

Pharmaceutical

Solvent-based APIs

Solvents handled

MethanolEthanolAcetoneHexaneDichloromethane

Information we need

What to send us for a quotation

We do not sell spray dryers from a fixed model list. Every dryer is sized to the material, so these are the details our engineers ask for first.

MaterialName, and what the powder is used for
FeedSolids content (%), viscosity, temperature, solvent (water or organic)
CapacityPowder output or water evaporation in kg/h, operating hours per day
Powder specFinal moisture, particle size range, bulk density
Heat sensitivityMaximum product temperature, if known
SiteAvailable heat source (steam, gas, electric, thermal oil) and building height

If you are not sure about a value, leave it blank and we will work it out with you, or test a sample.

FAQ

Questions about this dryer

Which solvents can be recovered?

Methanol, ethanol, isopropyl acetate, ethyl acetate, dichloromethane, acetone and hexane, among others. Tell us your solvent and we check compatibility.

Why use nitrogen?

Nitrogen keeps oxygen out, which prevents oxidation of the product and removes the explosion risk of solvent vapour in air.

Is it only for solvents?

It is also used for oxygen-sensitive products in water, where inert drying protects product quality.

Next step

Send us your material. We will size the dryer.

Tell us the material, solids content and the capacity you need. An engineer replies within one working day, and we can run a trial on your sample in our test center.